Information card for entry 7049106

Structure parameters

• Formula: C22 H36 Ni P
• Calculated formula: C22 H36 Ni P
• Title of publication: Simplified and versatile access to low valent Ni complexes by metal-free reduction of Ni^II precursors.
• Authors of publication: Moser, Emile; Jeanneau, Erwann; Mézailles, Nicolas; Olivier-Bourbigou, Hélène; Breuil, Pierre-Alain R
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 13
• Pages of publication: 4101 - 4104
• a: 9.5546 ± 0.001 Å
• b: 17.1029 ± 0.0015 Å
• c: 13.375 ± 0.0015 Å
• α: 90°
• β: 100 ± 0.01°
• γ: 90°
• Cell volume: 2152.4 ± 0.4 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for all reflections: 0.138
• Weighted residual factors for significantly intense reflections: 0.1096
• Weighted residual factors for all reflections included in the refinement: 0.138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0091
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No