Information card for entry 7049107

Structure parameters

• Formula: C18 H41 Ni O P Si2
• Calculated formula: C18 H41 Ni O P Si2
• Title of publication: Simplified and versatile access to low valent Ni complexes by metal-free reduction of Ni^II precursors.
• Authors of publication: Moser, Emile; Jeanneau, Erwann; Mézailles, Nicolas; Olivier-Bourbigou, Hélène; Breuil, Pierre-Alain R
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 13
• Pages of publication: 4101 - 4104
• a: 9.745 ± 0.008 Å
• b: 11.1357 ± 0.0011 Å
• c: 11.7289 ± 0.0011 Å
• α: 64.563 ± 0.009°
• β: 81.647 ± 0.007°
• γ: 80.817 ± 0.007°
• Cell volume: 1130.5 ± 0.9 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for all reflections: 0.0752
• Weighted residual factors for significantly intense reflections: 0.0605
• Weighted residual factors for all reflections included in the refinement: 0.0752
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9966
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No