Information card for entry 7049287

Structure parameters

• Formula: C42 H38 Cl2 F6 Ge2 N2 O6 P2 S2
• Calculated formula: C42 H38 Cl2 F6 Ge2 N2 O6 P2 S2
• Title of publication: Stabilization of bis(chlorogermyliumylidene)s within bifunctional PNNP ligand frameworks and their reactivity studies.
• Authors of publication: Sahoo, Padmini; Raut, Ravindra K.; Maurya, Devesh; Kumar, Vikas; Rani, Pooja; Gonnade, Rajesh G.; Majumdar, Moumita
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 21
• Pages of publication: 7344 - 7351
• a: 12.9761 ± 0.0012 Å
• b: 13.6739 ± 0.0014 Å
• c: 13.7965 ± 0.0012 Å
• α: 85.4 ± 0.006°
• β: 86.134 ± 0.006°
• γ: 70.497 ± 0.006°
• Cell volume: 2297.9 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1784
• Residual factor for significantly intense reflections: 0.0829
• Weighted residual factors for significantly intense reflections: 0.1585
• Weighted residual factors for all reflections included in the refinement: 0.1965
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No