Information card for entry 7049387

Structure parameters

• Chemical name: bis[(allyl)chloro(N-(diphenylboryl)-2-diphenylphosphanyl-benzaldimine)palladium]
• Formula: C68 H60 B2 Cl2 N2 P2 Pd2
• Calculated formula: C68 H60 B2 Cl2 N2 P2 Pd2
• Title of publication: Synthesis, structure and palladium coordination of ambiphilic, pyridine- and phosphine-tethered N-boryl imine ligands.
• Authors of publication: Lorenzini, Fabio; Lagueux-Tremblay, Pierre-Louis; Kayser, Laure V.; Anderson, Ethan; Arndtsen, Bruce A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5766 - 5772
• a: 10.9275 ± 0.0007 Å
• b: 15.5825 ± 0.001 Å
• c: 19.413 ± 0.0013 Å
• α: 96.589 ± 0.001°
• β: 104.476 ± 0.001°
• γ: 109.115 ± 0.001°
• Cell volume: 2953.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0906
• Weighted residual factors for all reflections included in the refinement: 0.0983
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No