Information card for entry 7049400

Structure parameters

• Formula: C98 H76 Cl5 Hg2 Li O4 P4
• Calculated formula: C98 H76 Cl5 Hg2 Li O4 P4
• Title of publication: Transmetallation of bis(6-diphenylphosphinoxy-acenapth-5-yl)mercury with tin tetrachloride, antimony trichloride and bismuth trichloride.
• Authors of publication: Olaru, Marian; Krupke, Sandra; Lork, Enno; Mebs, Stefan; Beckmann, Jens
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5585 - 5594
• a: 14.2748 ± 0.0008 Å
• b: 15.6725 ± 0.0008 Å
• c: 21.2164 ± 0.0011 Å
• α: 105.246 ± 0.002°
• β: 98.704 ± 0.002°
• γ: 94.464 ± 0.002°
• Cell volume: 4492.2 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0669
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1162
• Weighted residual factors for all reflections included in the refinement: 0.1216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No