Information card for entry 7049403

Structure parameters

• Formula: C24 H18 Cl Hg O P
• Calculated formula: C24 H18 Cl Hg O P
• Title of publication: Transmetallation of bis(6-diphenylphosphinoxy-acenapth-5-yl)mercury with tin tetrachloride, antimony trichloride and bismuth trichloride.
• Authors of publication: Olaru, Marian; Krupke, Sandra; Lork, Enno; Mebs, Stefan; Beckmann, Jens
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5585 - 5594
• a: 10.8014 ± 0.0004 Å
• b: 10.3777 ± 0.0004 Å
• c: 18.5406 ± 0.0008 Å
• α: 90°
• β: 105.655 ± 0.001°
• γ: 90°
• Cell volume: 2001.19 ± 0.14 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0212
• Residual factor for significantly intense reflections: 0.0198
• Weighted residual factors for significantly intense reflections: 0.0511
• Weighted residual factors for all reflections included in the refinement: 0.0516
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No