Information card for entry 7049664

Structure parameters

• Formula: C24 H12 F2 Mo O8 P2
• Calculated formula: C24 H12 F2 Mo O8 P2
• Title of publication: Ring size effects in cyclic fluorophosphites: ligands that span the bonding space between phosphites and PF3
• Authors of publication: Miles-Hobbs, Alexandra M.; Hunt, Eliza; Pringle, Paul. G.; Sparkes, Hazel A.
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 43.6028 ± 0.0006 Å
• b: 9.9809 ± 0.0002 Å
• c: 10.5817 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4605.1 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0148
• Residual factor for significantly intense reflections: 0.0145
• Weighted residual factors for significantly intense reflections: 0.0375
• Weighted residual factors for all reflections included in the refinement: 0.0376
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No