Information card for entry 7049665

Structure parameters

• Formula: C30 H20 F2 Mo O8 P2
• Calculated formula: C30 H20 F2 Mo O8 P2
• Title of publication: Ring size effects in cyclic fluorophosphites: ligands that span the bonding space between phosphites and PF3
• Authors of publication: Miles-Hobbs, Alexandra M.; Hunt, Eliza; Pringle, Paul. G.; Sparkes, Hazel A.
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 9.0915 ± 0.0003 Å
• b: 12.3578 ± 0.0005 Å
• c: 13.8479 ± 0.0005 Å
• α: 104.24 ± 0.002°
• β: 98.951 ± 0.003°
• γ: 100.618 ± 0.003°
• Cell volume: 1448.86 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0668
• Weighted residual factors for all reflections included in the refinement: 0.0719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No