Information card for entry 7049667

Structure parameters

• Formula: C26 H18 Mo O10 P2
• Calculated formula: C26 H18 Mo O10 P2
• Title of publication: Ring size effects in cyclic fluorophosphites: ligands that span the bonding space between phosphites and PF3
• Authors of publication: Miles-Hobbs, Alexandra M.; Hunt, Eliza; Pringle, Paul. G.; Sparkes, Hazel A.
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 8.257 ± 0.0002 Å
• b: 11.6685 ± 0.0003 Å
• c: 14.784 ± 0.0004 Å
• α: 69.956 ± 0.001°
• β: 76.943 ± 0.001°
• γ: 83.425 ± 0.001°
• Cell volume: 1302.45 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0278
• Residual factor for significantly intense reflections: 0.0238
• Weighted residual factors for significantly intense reflections: 0.0558
• Weighted residual factors for all reflections included in the refinement: 0.0577
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No