Information card for entry 7049666

Structure parameters

• Formula: C46 H29 Cl F4 O8 P4 Pt
• Calculated formula: C46 H29 Cl F4 O8 P4 Pt
• Title of publication: Ring size effects in cyclic fluorophosphites: ligands that span the bonding space between phosphites and PF3
• Authors of publication: Miles-Hobbs, Alexandra M.; Hunt, Eliza; Pringle, Paul. G.; Sparkes, Hazel A.
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 15.2985 ± 0.0004 Å
• b: 15.2985 ± 0.0004 Å
• c: 8.805 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2060.76 ± 0.1 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 85
• Hermann-Mauguin space group symbol: P 4/n
• Hall space group symbol: -P 4a
• Residual factor for all reflections: 0.0587
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0679
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No