Crystallography Open Database

Information card for entry 7049767

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Coordinates	7049767.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H27 B F4 P Sb
Calculated formula	C31 H27 B F4 P Sb
Title of publication	Phosphonium-stibonium and bis-stibonium cations as pnictogen-bonding catalysts for the transfer hydrogenation of quinolines.
Authors of publication	Yang, Mengxi; Hirai, Masato; Gabbaï, François P
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	20
Pages of publication	6685 - 6689
a	10.7939 ± 0.0005 Å
b	12.0638 ± 0.0005 Å
c	21.0206 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	2737.2 ± 0.2 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0404
Weighted residual factors for significantly intense reflections	0.085
Weighted residual factors for all reflections included in the refinement	0.0892
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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