Information card for entry 7049768

Structure parameters

• Formula: C37 H32 B2 F8 P Sb
• Calculated formula: C37 H32 B2 F8 P Sb
• Title of publication: Phosphonium-stibonium and bis-stibonium cations as pnictogen-bonding catalysts for the transfer hydrogenation of quinolines.
• Authors of publication: Yang, Mengxi; Hirai, Masato; Gabbaï, François P
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 20
• Pages of publication: 6685 - 6689
• a: 18.8422 ± 0.0017 Å
• b: 10.1309 ± 0.0009 Å
• c: 17.5792 ± 0.0017 Å
• α: 90°
• β: 93.042 ± 0.003°
• γ: 90°
• Cell volume: 3350.9 ± 0.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 99.98 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.205
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No