Information card for entry 7049793

Structure parameters

• Formula: C68 H67 Ag B2 F24 N4
• Calculated formula: C68 H67 Ag B2 F24 N4
• Title of publication: A d¹⁰ Ag(i) amine-borane σ-complex and comparison with a d⁸ Rh(i) analogue: structures on the η¹ to η²:η² continuum.
• Authors of publication: Johnson, Alice; Martínez-Martínez, Antonio J; Macgregor, Stuart A.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 26
• Pages of publication: 9776 - 9781
• a: 14.4114 ± 0.0002 Å
• b: 15.6413 ± 0.0003 Å
• c: 16.8798 ± 0.0003 Å
• α: 88.4148 ± 0.0013°
• β: 74.0062 ± 0.0014°
• γ: 78.2248 ± 0.0014°
• Cell volume: 3579.02 ± 0.11 ų
• Cell temperature: 150 ± 0.14 K
• Ambient diffraction temperature: 150 ± 0.14 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0334
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No