Information card for entry 7049794

Structure parameters

• Formula: C72 H70 B F24 N4 Rh
• Calculated formula: C72 H70 B F24 N4 Rh
• Title of publication: A d¹⁰ Ag(i) amine-borane σ-complex and comparison with a d⁸ Rh(i) analogue: structures on the η¹ to η²:η² continuum.
• Authors of publication: Johnson, Alice; Martínez-Martínez, Antonio J; Macgregor, Stuart A.; Weller, Andrew S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 26
• Pages of publication: 9776 - 9781
• a: 17.49982 ± 0.00019 Å
• b: 18.08188 ± 0.00017 Å
• c: 24.0311 ± 0.0003 Å
• α: 90°
• β: 106.971 ± 0.0011°
• γ: 90°
• Cell volume: 7273.03 ± 0.14 ų
• Cell temperature: 150.04 ± 0.18 K
• Ambient diffraction temperature: 150.04 ± 0.18 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1223
• Weighted residual factors for all reflections included in the refinement: 0.1369
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No