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Information card for entry 7049970
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Coordinates | 7049970.cif |
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Original paper (by DOI) | HTML |
Formula | C44 H64 N4 O Yb |
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Calculated formula | C44 H64 N4 O Yb |
Title of publication | Alternative (κ<sup>1</sup>-N:η<sup>6</sup>-arene vs.κ<sup>2</sup>-N,N) coordination of a sterically demanding amidinate ligand: are size and electronic structure of the Ln ion decisive factors? |
Authors of publication | Tolpygin, Aleksei O.; Shavyrin, Andrei S.; Cherkasov, Anton V.; Fukin, Georgy K.; Del Rosal, Iker; Maron, Laurent; Trifonov, Alexander A. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 23 |
Pages of publication | 8317 - 8326 |
a | 10.5855 ± 0.0001 Å |
b | 11.9856 ± 0.0001 Å |
c | 16.2221 ± 0.0002 Å |
α | 81.575 ± 0.001° |
β | 87.14 ± 0.001° |
γ | 77.417 ± 0.001° |
Cell volume | 1986.7 ± 0.04 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0272 |
Residual factor for significantly intense reflections | 0.0232 |
Weighted residual factors for significantly intense reflections | 0.0503 |
Weighted residual factors for all reflections included in the refinement | 0.0521 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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