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Information card for entry 7049971
Preview
Coordinates | 7049971.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C48 H73 I2 N4 O2 Yb |
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Calculated formula | C48 H73 I2 N4 O2 Yb |
Title of publication | Alternative (κ<sup>1</sup>-N:η<sup>6</sup>-arene vs.κ<sup>2</sup>-N,N) coordination of a sterically demanding amidinate ligand: are size and electronic structure of the Ln ion decisive factors? |
Authors of publication | Tolpygin, Aleksei O.; Shavyrin, Andrei S.; Cherkasov, Anton V.; Fukin, Georgy K.; Del Rosal, Iker; Maron, Laurent; Trifonov, Alexander A. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 23 |
Pages of publication | 8317 - 8326 |
a | 10.0868 ± 0.0007 Å |
b | 27.7319 ± 0.0018 Å |
c | 17.9352 ± 0.0012 Å |
α | 90° |
β | 90.184 ± 0.001° |
γ | 90° |
Cell volume | 5016.9 ± 0.6 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.039 |
Residual factor for significantly intense reflections | 0.0318 |
Weighted residual factors for significantly intense reflections | 0.0768 |
Weighted residual factors for all reflections included in the refinement | 0.0802 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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