Information card for entry 7050104

Structure parameters

• Formula: C87 H73 Ag3 B3 F12 N23 O2
• Calculated formula: C87 H73 Ag3 B3 F12 N23 O2
• Title of publication: Homo- and heteropolynuclear helicates with a ‘2 + 3 + 2’-dentate compartmental ligand
• Authors of publication: Argent, Stephen P.; Adams, Harry; Harding, Lindsay P.; Riis-Johannessen, T.; Jeffery, John C.; Ward, Michael D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2005
• Journal volume: 29
• Journal issue: 7
• Pages of publication: 904
• a: 28.943 ± 0.005 Å
• b: 11.5611 ± 0.0019 Å
• c: 25.405 ± 0.004 Å
• α: 90°
• β: 100.848 ± 0.003°
• γ: 90°
• Cell volume: 8349 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0969
• Weighted residual factors for all reflections included in the refinement: 0.1055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No