Information card for entry 7050105

Structure parameters

• Formula: C92 H79 Ag4 B4 F16 N25
• Calculated formula: C95 H70 Ag4 B4 F16 N22
• Title of publication: Homo- and heteropolynuclear helicates with a ‘2 + 3 + 2’-dentate compartmental ligand
• Authors of publication: Argent, Stephen P.; Adams, Harry; Harding, Lindsay P.; Riis-Johannessen, T.; Jeffery, John C.; Ward, Michael D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2005
• Journal volume: 29
• Journal issue: 7
• Pages of publication: 904
• a: 19.066 ± 0.003 Å
• b: 28.822 ± 0.004 Å
• c: 19.716 ± 0.003 Å
• α: 90°
• β: 115.093 ± 0.002°
• γ: 90°
• Cell volume: 9812 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2475
• Residual factor for significantly intense reflections: 0.1622
• Weighted residual factors for significantly intense reflections: 0.4759
• Weighted residual factors for all reflections included in the refinement: 0.5148
• Goodness-of-fit parameter for all reflections included in the refinement: 1.481
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No