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Information card for entry 7050718
Preview
Coordinates | 7050718.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H22 Br N7 Os |
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Calculated formula | C28 H22 Br N7 Os |
SMILES | [Os]123(Br)([n]4ccccc4N=[N]1c1ccccc1N2c1ccccc1)[n]1ccccc1N=[N]3c1ccccc1 |
Title of publication | Osmium(II) complexes of 2-[(arylamido)phenylazo]pyridines. New examples of deamination reactions—X-ray structure and redox propertiesElectronic supplementary information (ESI) available: partial energy level diagrams and molecular orbitals of 1a, 2a and 4a, UV-vis spectra of 4 complexes and cyclic voltammograms of 1b, 2b and 4b. See http://www.rsc.org/suppdata/nj/b1/b108507g/ |
Authors of publication | Das, Chayan; Peng, Shie-Ming; Lee, Gene-Hsiang; Goswami, Sreebrata |
Journal of publication | New Journal of Chemistry |
Year of publication | 2002 |
Journal volume | 26 |
Journal issue | 2 |
Pages of publication | 222 |
a | 13.643 ± 0.002 Å |
b | 14.1915 ± 0.0018 Å |
c | 13.85 ± 0.003 Å |
α | 90° |
β | 91.36 ± 0.02° |
γ | 90° |
Cell volume | 2680.8 ± 0.8 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0764 |
Residual factor for significantly intense reflections | 0.0353 |
Weighted residual factors for significantly intense reflections | 0.065 |
Weighted residual factors for all reflections included in the refinement | 0.0717 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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