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Information card for entry 7050719
Preview
Coordinates | 7050719.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H23 Br2 N7 Os |
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Calculated formula | C28 H23 Br2 N7 Os |
SMILES | [Os]12(Br)(Br)([n]3ccccc3N=[N]1c1ccccc1Nc1ccccc1)[n]1ccccc1N=[N]2c1ccccc1 |
Title of publication | Osmium(II) complexes of 2-[(arylamido)phenylazo]pyridines. New examples of deamination reactions—X-ray structure and redox propertiesElectronic supplementary information (ESI) available: partial energy level diagrams and molecular orbitals of 1a, 2a and 4a, UV-vis spectra of 4 complexes and cyclic voltammograms of 1b, 2b and 4b. See http://www.rsc.org/suppdata/nj/b1/b108507g/ |
Authors of publication | Das, Chayan; Peng, Shie-Ming; Lee, Gene-Hsiang; Goswami, Sreebrata |
Journal of publication | New Journal of Chemistry |
Year of publication | 2002 |
Journal volume | 26 |
Journal issue | 2 |
Pages of publication | 222 |
a | 38.4934 ± 0.0007 Å |
b | 38.4934 ± 0.0007 Å |
c | 9.7379 ± 0.0002 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 12495.9 ± 0.4 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 1 K |
Number of distinct elements | 5 |
Space group number | 148 |
Hermann-Mauguin space group symbol | R -3 :H |
Hall space group symbol | -R 3 |
Residual factor for all reflections | 0.0399 |
Residual factor for significantly intense reflections | 0.0285 |
Weighted residual factors for all reflections | 0.0726 |
Weighted residual factors for significantly intense reflections | 0.0611 |
Goodness-of-fit parameter for all reflections | 1.15 |
Goodness-of-fit parameter for significantly intense reflections | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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