Information card for entry 7050797

Structure parameters

• Formula: C6 H16 Cl4 Ge N2
• Calculated formula: C6 H16 Cl4 Ge N2
• SMILES: [Ge]1(Cl)(Cl)(Cl)(Cl)[N](C)(C)CC[N]1(C)C
• Title of publication: Syntheses of new hexacoordinate germanium(IV) complexes. Crystal structures and properties of [GeCl4(TMEDA)] and [GeCl2(N3)2(TMEDA)]
• Authors of publication: Ejfler, Jolanta; Szafert, Slawomir; Jiao, Haijun; Sobota, Piotr
• Journal of publication: New Journal of Chemistry
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 6
• Pages of publication: 803
• a: 14.633 ± 0.002 Å
• b: 7.328 ± 0.003 Å
• c: 11.725 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1257.3 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.1642
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No