Information card for entry 7050798

Structure parameters

• Formula: C6 H16 Cl2 Ge N8
• Calculated formula: C6 H16 Cl2 Ge N8
• SMILES: C[N]1(C)CC[N]([Ge]1(N=N#N)(Cl)(N=N#N)Cl)(C)C
• Title of publication: Syntheses of new hexacoordinate germanium(IV) complexes. Crystal structures and properties of [GeCl4(TMEDA)] and [GeCl2(N3)2(TMEDA)]
• Authors of publication: Ejfler, Jolanta; Szafert, Slawomir; Jiao, Haijun; Sobota, Piotr
• Journal of publication: New Journal of Chemistry
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 6
• Pages of publication: 803
• a: 8.57 ± 0.002 Å
• b: 13.35 ± 0.003 Å
• c: 12.227 ± 0.002 Å
• α: 90°
• β: 108.63 ± 0.03°
• γ: 90°
• Cell volume: 1325.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.102
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No