Information card for entry 7051013

Structure parameters

• Common name: Allyltropp-methyltropp-rhodium
• Formula: C56.5 H45.5 Cl1.5 P2 Rh
• Calculated formula: C56.5 H45.5 Cl1.5 P2 Rh
• Title of publication: Highly distorted d8-rhodium(+I) and d10-rhodium(-I) complexes: synthesis, reactivity, and structures in solution and solid state
• Authors of publication: Deblon, Stephan; Rüegger, Heinz; Schönberg, Hartmut; Loss, Sandra; Gramlich, Volker; Grützmacher, Hansjörg
• Journal of publication: New Journal of Chemistry
• Year of publication: 2001
• Journal volume: 25
• Journal issue: 1
• Pages of publication: 83
• a: 45.899 ± 0.051 Å
• b: 10.159 ± 0.01 Å
• c: 19.773 ± 0.019 Å
• α: 90°
• β: 102.27 ± 0.08°
• γ: 90°
• Cell volume: 9009 ± 16 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for all reflections: 0.1218
• Weighted residual factors for significantly intense reflections: 0.1132
• Goodness-of-fit parameter for all reflections: 1.073
• Goodness-of-fit parameter for significantly intense reflections: 1.122
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No