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Information card for entry 7052392
Preview
Coordinates | 7052392.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Bis(potassium-(4,7,13,1621,24-Hexaoxa-1,10- diazabicyclo(8.8.8)hexacosane))-nonagermanid - ammonia(1/4) |
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Chemical name | Bis[potassium-(4,7,13,1621,24-Hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane)]- nonagermanid - ammonia(1/4) |
Formula | C36 H84 Ge5 K2 N8 O12 |
Calculated formula | C36 H84 Ge5 K2 N8 O12 |
SMILES | [Ge]12[Ge]34[Ge]51[Ge]23[Ge]45.[K]1234567[O]8CC[O]3CC[N]37CC[O]5CC[O]4CC[N]6(CC[O]2CC[O]1CC3)CC8.[K]1234567[O]8CC[O]2CC[N]27CC[O]4CC[O]3CC[N]6(CC[O]5CC[O]1CC2)CC8.N.N.N.N |
Title of publication | Ge52? Zintl anions: synthesis and crystal structures of [K([2.2.2]-crypt)]2Ge5?4NH3 and [Rb([2.2.2]-crypt)]2Ge5?4NH3 |
Authors of publication | Suchentrunk, Christof; Korber, Nikolaus |
Journal of publication | New Journal of Chemistry |
Year of publication | 2006 |
Journal volume | 30 |
Journal issue | 12 |
Pages of publication | 1737 |
a | 11.2887 ± 0.0009 Å |
b | 11.8949 ± 0.0009 Å |
c | 11.9433 ± 0.0009 Å |
α | 117.911 ± 0.008° |
β | 98.65 ± 0.009° |
γ | 91.797 ± 0.009° |
Cell volume | 1391.5 ± 0.2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 6 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0501 |
Residual factor for significantly intense reflections | 0.0449 |
Weighted residual factors for significantly intense reflections | 0.1181 |
Weighted residual factors for all reflections included in the refinement | 0.1205 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7052392.html
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