Information card for entry 7052393

Structure parameters

• Common name: Bis(rubidium-(4,7,13,1621,24-Hexaoxa-1,10- diazabicyclo(8.8.8)hexacosane))-nonagermanid - ammonia(1/4)
• Chemical name: Bis[rubidium-(4,7,13,1621,24-Hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane)]- nonagermanid - ammonia(1/4)
• Formula: C36 H84 Ge5 N8 O12 Rb2
• Calculated formula: C36 H84 Ge5 N8 O12 Rb2
• Title of publication: Ge52? Zintl anions: synthesis and crystal structures of [K([2.2.2]-crypt)]2Ge5?4NH3 and [Rb([2.2.2]-crypt)]2Ge5?4NH3
• Authors of publication: Suchentrunk, Christof; Korber, Nikolaus
• Journal of publication: New Journal of Chemistry
• Year of publication: 2006
• Journal volume: 30
• Journal issue: 12
• Pages of publication: 1737
• a: 11.3169 ± 0.0015 Å
• b: 12.3333 ± 0.0015 Å
• c: 20.915 ± 0.003 Å
• α: 89.183 ± 0.013°
• β: 83.6 ± 0.02°
• γ: 78.266 ± 0.015°
• Cell volume: 2840.3 ± 0.7 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.0946
• Weighted residual factors for all reflections included in the refinement: 0.1013
• Goodness-of-fit parameter for all reflections included in the refinement: 0.883
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No