Information card for entry 7055843

Structure parameters

• Formula: C46 H104 Eu2 N12 Si4
• Calculated formula: C46 H104 Eu2 N12 Si4
• Title of publication: Synthesis and molecular structures of divalent bridged bis(guanidinate) europium complexes and their application in intermolecular hydrophosphination of alkenes and alkynes
• Authors of publication: Liu, Qianqian; Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Yao, Yingming; Zhang, Yong; Shen, Qi
• Journal of publication: New J. Chem.
• Year of publication: 2016
• Journal volume: 40
• Journal issue: 12
• Pages of publication: 10447
• a: 13.5784 ± 0.0013 Å
• b: 13.6097 ± 0.001 Å
• c: 19.0544 ± 0.001 Å
• α: 71.442 ± 0.01°
• β: 75.023 ± 0.009°
• γ: 83.412 ± 0.012°
• Cell volume: 3222.7 ± 0.5 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1289
• Residual factor for significantly intense reflections: 0.0851
• Weighted residual factors for significantly intense reflections: 0.1607
• Weighted residual factors for all reflections included in the refinement: 0.1836
• Goodness-of-fit parameter for all reflections included in the refinement: 1.133
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No