Information card for entry 7055844

Structure parameters

• Formula: C64 H104 Eu2 N12 O4
• Calculated formula: C64 H104 Eu2 N12 O4
• Title of publication: Synthesis and molecular structures of divalent bridged bis(guanidinate) europium complexes and their application in intermolecular hydrophosphination of alkenes and alkynes
• Authors of publication: Liu, Qianqian; Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Yao, Yingming; Zhang, Yong; Shen, Qi
• Journal of publication: New J. Chem.
• Year of publication: 2016
• Journal volume: 40
• Journal issue: 12
• Pages of publication: 10447
• a: 12.834 ± 0.004 Å
• b: 14.323 ± 0.004 Å
• c: 19.638 ± 0.007 Å
• α: 90°
• β: 107.298 ± 0.006°
• γ: 90°
• Cell volume: 3446.6 ± 1.9 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.1115
• Weighted residual factors for all reflections included in the refinement: 0.1233
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No