Information card for entry 7055845

Structure parameters

• Formula: C35 H76 Cl Eu N6 O3 Si2
• Calculated formula: C35 H76 Cl Eu N6 O3 Si2
• Title of publication: Synthesis and molecular structures of divalent bridged bis(guanidinate) europium complexes and their application in intermolecular hydrophosphination of alkenes and alkynes
• Authors of publication: Liu, Qianqian; Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Yao, Yingming; Zhang, Yong; Shen, Qi
• Journal of publication: New J. Chem.
• Year of publication: 2016
• Journal volume: 40
• Journal issue: 12
• Pages of publication: 10447
• a: 14.6965 ± 0.0005 Å
• b: 13.2218 ± 0.0004 Å
• c: 23.7134 ± 0.0008 Å
• α: 90°
• β: 92.135 ± 0.003°
• γ: 90°
• Cell volume: 4604.7 ± 0.3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0931
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1869
• Weighted residual factors for all reflections included in the refinement: 0.2072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No