Information card for entry 7057143

Structure parameters

• Formula: C48.5 H59 Cl N11
• Calculated formula: C48.5 H59 Cl N11
• Title of publication: Synthesis of novel series of 7,7′-(substituted methylene)bis-imidazo[1,2-b]pyrazoles via an acid catalyzed one-pot three-component reaction
• Authors of publication: Driowya, Mohsine; Allouchi, Hassan; Gally, José Manuel; Bonnet, Pascal; Guillaumet, Gérald
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 8
• Pages of publication: 5728
• a: 11.8594 ± 0.0006 Å
• b: 13.3077 ± 0.0007 Å
• c: 15.7675 ± 0.0008 Å
• α: 105.058 ± 0.004°
• β: 101.304 ± 0.004°
• γ: 96.287 ± 0.004°
• Cell volume: 2322.3 ± 0.2 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1634
• Residual factor for significantly intense reflections: 0.0924
• Weighted residual factors for significantly intense reflections: 0.2518
• Weighted residual factors for all reflections included in the refinement: 0.3208
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No