Information card for entry 7057297

Structure parameters

• Formula: C26 H34 Au B Cl O2 P
• Calculated formula: C26 H34 Au B Cl O2 P
• Title of publication: Regiospecific and stereoselective synthesis of (E)- and (Z)-2-phosphino-1-alkenyl boronates via Cu-catalyzed hydroboration of alkynylphosphines
• Authors of publication: Song, Liubing; Ma, Xufeng; Xu, Sheng; Shi, Min; Zhang, Jun
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 11
• Pages of publication: 8342
• a: 11.9069 ± 0.0009 Å
• b: 15.0564 ± 0.001 Å
• c: 22.5926 ± 0.0015 Å
• α: 88.786 ± 0.003°
• β: 79.733 ± 0.003°
• γ: 82.636 ± 0.003°
• Cell volume: 3952.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0339
• Weighted residual factors for significantly intense reflections: 0.0778
• Weighted residual factors for all reflections included in the refinement: 0.0826
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No