Information card for entry 7057298

Structure parameters

• Formula: C26 H28 B O2 P
• Calculated formula: C26 H28 B O2 P
• Title of publication: Regiospecific and stereoselective synthesis of (E)- and (Z)-2-phosphino-1-alkenyl boronates via Cu-catalyzed hydroboration of alkynylphosphines
• Authors of publication: Song, Liubing; Ma, Xufeng; Xu, Sheng; Shi, Min; Zhang, Jun
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 11
• Pages of publication: 8342
• a: 11.42 ± 0.014 Å
• b: 7.124 ± 0.01 Å
• c: 29.97 ± 0.03 Å
• α: 90°
• β: 94.83 ± 0.03°
• γ: 90°
• Cell volume: 2430 ± 5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0867
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.1706
• Weighted residual factors for all reflections included in the refinement: 0.197
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No