Information card for entry 7057557

Structure parameters

• Formula: C28 H39 Cu N4 O2.5
• Calculated formula: C28 H39 Cu N4 O2.5
• Title of publication: Synthesis and crystal structures of salen-type Cu(ii) and Ni(ii) Schiff base complexes: application in [3+2]-cycloaddition and A3-coupling reactions
• Authors of publication: Agrahari, Bhumika; Layek, Samaresh; Ganguly, Rakesh; Pathak, Devendra D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 16
• Pages of publication: 13754
• a: 9.461 ± 0.0011 Å
• b: 15.3673 ± 0.0017 Å
• c: 19.021 ± 0.002 Å
• α: 92.716 ± 0.003°
• β: 93.956 ± 0.003°
• γ: 102.009 ± 0.003°
• Cell volume: 2693.1 ± 0.5 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1722
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for significantly intense reflections: 0.1363
• Weighted residual factors for all reflections included in the refinement: 0.1721
• Goodness-of-fit parameter for all reflections included in the refinement: 0.936
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No