Information card for entry 7057558

Structure parameters

• Formula: C28 H38 N4 Ni O2
• Calculated formula: C28 H38 N4 Ni O2
• Title of publication: Synthesis and crystal structures of salen-type Cu(ii) and Ni(ii) Schiff base complexes: application in [3+2]-cycloaddition and A3-coupling reactions
• Authors of publication: Agrahari, Bhumika; Layek, Samaresh; Ganguly, Rakesh; Pathak, Devendra D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 16
• Pages of publication: 13754
• a: 12.0046 ± 0.0013 Å
• b: 8.5202 ± 0.0009 Å
• c: 26.095 ± 0.002 Å
• α: 90°
• β: 92.104 ± 0.009°
• γ: 90°
• Cell volume: 2667.2 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1134
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.1138
• Weighted residual factors for all reflections included in the refinement: 0.1357
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No