Information card for entry 7058431

Structure parameters

• Formula: C55 H75 P Th
• Calculated formula: C55 H75 P Th
• Title of publication: Preparation of a potassium chloride bridged thorium phosphinidiide complex and its reactivity towards small organic molecules
• Authors of publication: Wang, Yongsong; Zhang, Congcong; Zi, Guofu; Ding, Wanjian; Walter, Marc D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 24
• Pages of publication: 9527
• a: 11.9928 ± 0.0004 Å
• b: 17.9174 ± 0.0007 Å
• c: 24.0867 ± 0.0008 Å
• α: 90°
• β: 102.409 ± 0.004°
• γ: 90°
• Cell volume: 5054.8 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0627
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections included in the refinement: 0.0673
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No