Information card for entry 7058432

Structure parameters

• Formula: C45 H71 N2 P Th
• Calculated formula: C45 H71 N2 P Th
• Title of publication: Preparation of a potassium chloride bridged thorium phosphinidiide complex and its reactivity towards small organic molecules
• Authors of publication: Wang, Yongsong; Zhang, Congcong; Zi, Guofu; Ding, Wanjian; Walter, Marc D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 24
• Pages of publication: 9527
• a: 19.0237 ± 0.0007 Å
• b: 10.9583 ± 0.0003 Å
• c: 22.7751 ± 0.0009 Å
• α: 90°
• β: 110.359 ± 0.004°
• γ: 90°
• Cell volume: 4451.3 ± 0.3 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0619
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.0567
• Weighted residual factors for all reflections included in the refinement: 0.0645
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No