Information card for entry 7059465

Structure parameters

• Formula: C56 H58 Cl4 N4 O6 P2 Re2
• Calculated formula: C56 H58 Cl4 N4 O6 P2 Re2
• SMILES: [Re]1(Cl)(Cl)([P](c2ccccc2)(c2ccccc2)c2ccccc2)(OC(=N[N]1=C(C)C)c1cc(ccc1)C1O[Re](Cl)(Cl)([P](c2ccccc2)(c2ccccc2)c2ccccc2)(=O)[N](N=1)=C(C)C)=O.O=C(C)C.O=C(C)C
• Title of publication: The reaction of oxidorhenium(v) with dipodal and tripodal aroylhydrazines: formation of dinuclear and trinuclear aroylhydrazone-bridged rhenium(v) complexes
• Authors of publication: Mukiza, Janvier; Blacque, Olivier; Habarurema, Gratien; Kampire, Edwige
• Journal of publication: New Journal of Chemistry
• Year of publication: 2020
• Journal volume: 44
• Journal issue: 17
• Pages of publication: 7080 - 7090
• a: 15.75942 ± 0.00009 Å
• b: 14.2297 ± 0.00007 Å
• c: 25.4385 ± 0.00012 Å
• α: 90°
• β: 98.728 ± 0.0005°
• γ: 90°
• Cell volume: 5638.57 ± 0.05 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0359
• Weighted residual factors for significantly intense reflections: 0.0985
• Weighted residual factors for all reflections included in the refinement: 0.0992
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No