Information card for entry 7059466

Structure parameters

• Formula: C79.25 H82.64 Br4.15 Cl1.65 N6 O8.9 P2.9 Re2.9
• Calculated formula: C70.2378 H64.6294 Br4.146 Cl1.662 N6 O5.9021 P2.9021 Re2.9021
• Title of publication: The reaction of oxidorhenium(v) with dipodal and tripodal aroylhydrazines: formation of dinuclear and trinuclear aroylhydrazone-bridged rhenium(v) complexes
• Authors of publication: Mukiza, Janvier; Blacque, Olivier; Habarurema, Gratien; Kampire, Edwige
• Journal of publication: New Journal of Chemistry
• Year of publication: 2020
• Journal volume: 44
• Journal issue: 17
• Pages of publication: 7080 - 7090
• a: 19.7456 ± 0.0005 Å
• b: 15.7521 ± 0.0004 Å
• c: 26.807 ± 0.0007 Å
• α: 90°
• β: 96.356 ± 0.003°
• γ: 90°
• Cell volume: 8286.7 ± 0.4 ų
• Cell temperature: 160 ± 1 K
• Ambient diffraction temperature: 160 ± 1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0371
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No