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Information card for entry 7059813
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Coordinates | 7059813.cif |
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Original paper (by DOI) | HTML |
Chemical name | 4-hydroxy-1,4-bis(4-methoxyphenyl)butan-1-one |
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Formula | C18 H20 O4 |
Calculated formula | C18 H20 O4 |
Title of publication | Preparation of aromatic γ-hydroxyketones by means of Heck coupling of aryl halides and 2,3-dihydrofuran, catalyzed by a palladium(ii) glycine complex under microwave irradiation |
Authors of publication | Jiménez-Cruz, Juan C.; Guzmán-Mejía, Ramón; Juaristi, Eusebio; Sánchez-Antonio, Omar; García-Revilla, Marco A.; González-Campos, J. Betzabe; Aviña-Verduzco, Judit |
Journal of publication | New Journal of Chemistry |
Year of publication | 2020 |
Journal volume | 44 |
Journal issue | 31 |
Pages of publication | 13382 - 13392 |
a | 11.1124 ± 0.0005 Å |
b | 5.2113 ± 0.0002 Å |
c | 13.3792 ± 0.0006 Å |
α | 90° |
β | 93.648 ± 0.002° |
γ | 90° |
Cell volume | 773.22 ± 0.06 Å3 |
Cell temperature | 273.15 K |
Ambient diffraction temperature | 273.15 K |
Number of distinct elements | 3 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0584 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for significantly intense reflections | 0.1337 |
Weighted residual factors for all reflections included in the refinement | 0.1434 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7059813.html
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