Information card for entry 7059814

Structure parameters

• Common name: GliPdCl2
• Chemical name: Trans-dichlorobis(2-methoxy-2-oxoethyl)azanidepalladium(II)
• Formula: C6 H14 Cl2 N2 O4 Pd
• Calculated formula: C6 H14 Cl2 N2 O4 Pd
• Title of publication: Preparation of aromatic γ-hydroxyketones by means of Heck coupling of aryl halides and 2,3-dihydrofuran, catalyzed by a palladium(ii) glycine complex under microwave irradiation
• Authors of publication: Jiménez-Cruz, Juan C.; Guzmán-Mejía, Ramón; Juaristi, Eusebio; Sánchez-Antonio, Omar; García-Revilla, Marco A.; González-Campos, J. Betzabe; Aviña-Verduzco, Judit
• Journal of publication: New Journal of Chemistry
• Year of publication: 2020
• Journal volume: 44
• Journal issue: 31
• Pages of publication: 13382 - 13392
• a: 9.0537 ± 0.0003 Å
• b: 12.166 ± 0.0004 Å
• c: 5.4933 ± 0.0002 Å
• α: 90°
• β: 96.599 ± 0.001°
• γ: 90°
• Cell volume: 601.06 ± 0.04 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0505
• Weighted residual factors for all reflections included in the refinement: 0.0532
• Goodness-of-fit parameter for all reflections included in the refinement: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No