Information card for entry 7060484

Structure parameters

• Formula: C14 H9 N O5 S2 W
• Calculated formula: C14 H9 N O5 S2 W
• Title of publication: Synthesis and structure of thienyl Fischer carbene complexes of PtII for application in alkyne hydrosilylation
• Authors of publication: Lamprecht, Zandria; Malan, Frederick P.; Lotz, Simon; Bezuidenhout, Daniela I.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2021
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6220 - 6230
• a: 6.5766 ± 0.001 Å
• b: 14.83 ± 0.002 Å
• c: 17.779 ± 0.003 Å
• α: 103 ± 0.008°
• β: 94.315 ± 0.007°
• γ: 90.165 ± 0.007°
• Cell volume: 1684.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0848
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1134
• Weighted residual factors for all reflections included in the refinement: 0.1241
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No