Information card for entry 7061789

Structure parameters

• Formula: C14 H25 Cl2 N2 Ni P
• Calculated formula: C14 H25 Cl2 N2 Ni P
• Title of publication: High-spin, tetrahedral cobalt(ii) and nickel(ii) complexes supported by monoprotic aminophosphine ligands, and attempted extension to copper(ii) complexes: synthesis, characterization, and unexpected reactivity
• Authors of publication: Kelly, Jordan C.; Bloomfield, Aaron J.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2022
• Journal volume: 46
• Journal issue: 39
• Pages of publication: 18647 - 18651
• a: 13.3712 ± 0.001 Å
• b: 12.0474 ± 0.0009 Å
• c: 23.5918 ± 0.0018 Å
• α: 90°
• β: 104.837 ± 0.004°
• γ: 90°
• Cell volume: 3673.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0486
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0785
• Weighted residual factors for all reflections included in the refinement: 0.0869
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No