Information card for entry 7061790

Structure parameters

• Formula: C14 H26 Cl3 Cu N2 O P
• Calculated formula: C14 H26 Cl3 Cu N2 O P
• Title of publication: High-spin, tetrahedral cobalt(ii) and nickel(ii) complexes supported by monoprotic aminophosphine ligands, and attempted extension to copper(ii) complexes: synthesis, characterization, and unexpected reactivity
• Authors of publication: Kelly, Jordan C.; Bloomfield, Aaron J.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2022
• Journal volume: 46
• Journal issue: 39
• Pages of publication: 18647 - 18651
• a: 14.1431 ± 0.0001 Å
• b: 8.9812 ± 0.0001 Å
• c: 17.4366 ± 0.0002 Å
• α: 90°
• β: 101.168 ± 0.001°
• γ: 90°
• Cell volume: 2172.89 ± 0.04 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0644
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1361
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No