Crystallography Open Database

Information card for entry 7062234

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Coordinates	7062234.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H64 Bi2 K N2 O6 Rh2
Calculated formula	C37 H64 Bi2 K N2 O6 Rh2
Title of publication	Capture of [Bi4]6− and [Bi3]5− anions by [Rh(L)]+ (L = COD) cations in the closo heteroatomic clusters {Bi4[Rh(L)]4}2− and {Bi3[Rh(L)]3}2−
Authors of publication	Liang, Zhibing; Lin, Lifang; Liang, Yuanwei; Wang, Yi
Journal of publication	New Journal of Chemistry
Year of publication	2023
Journal volume	47
Journal issue	8
Pages of publication	3993 - 3998
a	13.6378 ± 0.0007 Å
b	17.7192 ± 0.0009 Å
c	17.8331 ± 0.0009 Å
α	90°
β	92.0637 ± 0.0009°
γ	90°
Cell volume	4306.6 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0499
Residual factor for significantly intense reflections	0.0357
Weighted residual factors for significantly intense reflections	0.0652
Weighted residual factors for all reflections included in the refinement	0.0682
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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