Information card for entry 7062235

Structure parameters

• Formula: C61 H112 Bi3 K2 N5 O12 Rh3
• Calculated formula: C61 H112 Bi3 K2 N5 O12 Rh3
• Title of publication: Capture of [Bi4]6− and [Bi3]5− anions by [Rh(L)]+ (L = COD) cations in the closo heteroatomic clusters {Bi4[Rh(L)]4}2− and {Bi3[Rh(L)]3}2−
• Authors of publication: Liang, Zhibing; Lin, Lifang; Liang, Yuanwei; Wang, Yi
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 8
• Pages of publication: 3993 - 3998
• a: 10.8655 ± 0.0006 Å
• b: 14.0066 ± 0.0008 Å
• c: 24.6791 ± 0.0014 Å
• α: 85.315 ± 0.002°
• β: 77.69 ± 0.002°
• γ: 84.06 ± 0.002°
• Cell volume: 3642.9 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0261
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for significantly intense reflections: 0.0536
• Weighted residual factors for all reflections included in the refinement: 0.0547
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.41328 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No