Information card for entry 7063467

Structure parameters

• Formula: C33 H54 N4 O Si4 U
• Calculated formula: C33 H54 N4 O Si4 U
• Title of publication: Advancing understanding of comparison of M-O covalency in isostructural M-OSiMe3 (M = Ce, Th, U) complexes
• Authors of publication: Liu, Kang; Chi, Xiao-Wang; Guo, Yan; Hu, Kongqiu; Mei, Lei; Yu, Jipan; Shi, Weiqun
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• a: 17.171 ± 0.004 Å
• b: 17.171 ± 0.004 Å
• c: 23.79 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6075 ± 3 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 6
• Space group number: 161
• Hermann-Mauguin space group symbol: R 3 c :H
• Hall space group symbol: R 3 -2"c
• Residual factor for all reflections: 0.0212
• Residual factor for significantly intense reflections: 0.0144
• Weighted residual factors for significantly intense reflections: 0.0326
• Weighted residual factors for all reflections included in the refinement: 0.0336
• Goodness-of-fit parameter for all reflections included in the refinement: 0.892
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No