Information card for entry 7100778

Structure parameters

• Formula: C52.5 H77 N3 Na O2 Si2 Sm
• Calculated formula: C52.5 H73 N3 Na O2 Si2 Sm
• Title of publication: C-H Activation (g-deprotonation) of a Sm(III) bis(trimethylsilyl)amide complex via macrocyclic stabilisation of the sodium counter ion
• Authors of publication: Michael Guy Gardiner; Jun Wang
• Journal of publication: Chemical Communications
• Year of publication: 2005
• a: 11.8735 ± 0.0001 Å
• b: 12.4181 ± 0.0002 Å
• c: 18.6506 ± 0.0002 Å
• α: 88.074 ± 0.0006°
• β: 89.2062 ± 0.0006°
• γ: 70.8546 ± 0.0004°
• Cell volume: 2596.38 ± 0.05 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No