Information card for entry 7102146

Structure parameters

• Formula: C86 H124 N4 O2 Pb2
• Calculated formula: C86 H124 N4 O2 Pb2
• SMILES: [Pb]1(Oc2c(cccc2C(C)(C)C)C(C)(C)C)[N](=C(C)C=C(N1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: A new type of heteroleptic complex of divalent lead and synthesis of the P-plumbyleniophosphasilene, R2Si=P‒Pb(L): (L = β-diketiminate)
• Authors of publication: Yao, Shenglai; Block, Stefan; Brym, Markus; Driess, Matthias
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 37
• Pages of publication: 3844 - 3846
• a: 19.6849 ± 0.0006 Å
• b: 10.9636 ± 0.0004 Å
• c: 36.7625 ± 0.0012 Å
• α: 90°
• β: 91.304 ± 0.001°
• γ: 90°
• Cell volume: 7931.9 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1122
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No