Information card for entry 7102147

Structure parameters

• Formula: C38 H66 N3 Pb Si2
• Calculated formula: C38 H66 N3 Pb Si2
• Title of publication: A new type of heteroleptic complex of divalent lead and synthesis of the P-plumbyleniophosphasilene, R2Si=P‒Pb(L): (L = β-diketiminate)
• Authors of publication: Yao, Shenglai; Block, Stefan; Brym, Markus; Driess, Matthias
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2007
• Journal issue: 37
• Pages of publication: 3844 - 3846
• a: 11.9877 ± 0.0007 Å
• b: 12.6789 ± 0.0008 Å
• c: 15.152 ± 0.001 Å
• α: 76.037 ± 0.002°
• β: 89.319 ± 0.002°
• γ: 65.115 ± 0.002°
• Cell volume: 2016.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0713
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1674
• Weighted residual factors for all reflections included in the refinement: 0.1809
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No