Information card for entry 7102686

Structure parameters

• Formula: C102 H64 B2 Cl12 F48 Pd3
• Calculated formula: C134 H84 B2 Cl12 F48 Pd5
• Title of publication: Stepwise growth of polypalladium chains in 1,4-diphenyl-1,3-butadiene sandwich complexes.
• Authors of publication: Tatsumi, Yasuki; Naga, Tomoki; Nakashima, Hiromitsu; Murahashi, Tetsuro; Kurosawa, Hideo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 12
• Pages of publication: 1430 - 1431
• a: 17.981 ± 0.002 Å
• b: 12.556 ± 0.005 Å
• c: 26.639 ± 0.005 Å
• α: 90°
• β: 102.91 ± 0.01°
• γ: 90°
• Cell volume: 5861 ± 2 ų
• Cell temperature: 223.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0872
• Weighted residual factors for all reflections included in the refinement: 0.081
• Goodness-of-fit parameter for all reflections included in the refinement: 2.471
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No