Information card for entry 7102687

Structure parameters

• Formula: C34 H32 B2 Cl2 F8 Pd2
• Calculated formula: C68 H64 B2 Cl4 F8 Pd4
• Title of publication: Stepwise growth of polypalladium chains in 1,4-diphenyl-1,3-butadiene sandwich complexes.
• Authors of publication: Tatsumi, Yasuki; Naga, Tomoki; Nakashima, Hiromitsu; Murahashi, Tetsuro; Kurosawa, Hideo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2004
• Journal issue: 12
• Pages of publication: 1430 - 1431
• a: 20.479 ± 0.001 Å
• b: 7.9523 ± 0.0004 Å
• c: 22.452 ± 0.002 Å
• α: 90°
• β: 114.108 ± 0.002°
• γ: 90°
• Cell volume: 3337.4 ± 0.4 ų
• Cell temperature: 213.2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for all reflections included in the refinement: 0.0674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No